It might be worth combining these files in Pointless before Scala to
check that they are compatible
Phil
On 15 May 2009, at 14:28, Rita GIORDANO wrote:
> Dear all,
> I have 8 data set from insulin at 1.2 A, after used Mosflm and Scala
> I used tha program Sortmtz to reset the batch number, first, and
> after unsorted MTZ files in one mtz file.
> When I put this mtz file in SCALA I have the follow error message:
>
> **** Insufficient data to determine parameters ****
> 0 reflections, 138 parameters
>
> Scala: *** Too few reflections ***
> Times: User: 30.2s System: 0.6s Elapsed: 0:31 </pre>
> </html>
> ***************************************************************************
> * Information from CCP4Interface script
> ***************************************************************************
> The program run with command: scala HKLIN "/home/rgiordan/
> sortInsulin/prova7.mtz" HKLOUT "/home/rgiordan/sortInsulin/
> sortInsulin_38_1_mtz.tmp" SCALES "/home/rgiordan/sortInsulin/
> sortInsulin_38.scala" ROGUES "/home/rgiordan/sortInsulin/
> sortInsulin_38_rogues.log" NORMPLOT "/home/rgiordan/sortInsulin/
> sortInsulin_38_normplot.xmgr" ANOMPLOT "/home/rgiordan/sortInsulin/
> sortInsulin_38_anomplot.xmgr" PLOT "/home/rgiordan/sortInsulin/
> sortInsulin_38_surface_plot.plt" CORRELPLOT "/home/rgiordan/
> sortInsulin/sortInsulin_38_correlplot.xmgr"
> has failed with error message
> Scala: *** Too few reflections ***
> ***************************************************************************
>
>
> #CCP4I TERMINATION STATUS 0 " Scala: *** Too few reflections ***"
> #CCP4I TERMINATION TIME 14 May 2009 14:59:13
> #CCP4I MESSAGE Task failed
>
> I tried to merge only the first 5 mtz files and SCALA works
> properly, after I processed the latest 3 and everything is ok, but
> when I use the 8 files together i have problem.
> Somebody know why I have this kind of problem?
> Thank in advance.
> Best regards,
> Rita Giordano
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