Dear Chandra
SLS and ourselves (SOLEIL) are dealing rather often with large unit cells and fancy crystal orientations. No great secret, and things have already been mentioned: combining three-axis goniometry, large area Pixel detector, low background, small wedges and/or helical scans, Staraniso...
This works pretty well at SOLEIL, and I do know it works probably better at SLS. We can discuss off-line about more details if you wish.
Best.
leo
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Leonard Chavas
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Synchrotron SOLEIL
Proxima-I
L'Orme des Merisiers
Saint-Aubin - BP 48
91192 Gif-sur-Yvette Cedex
France
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Phone: +33 169 359 746
Mobile: +33 644 321 614
E-mail: [log in to unmask]
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> On 21 Aug 2019, at 21:47, Frank Von Delft <[log in to unmask]> wrote:
>
> We also described how to bend the loops in this article: http://doi.org/gcb8j3 Figure 4 specifically.
>
>
> On 21/08/2019 18:21, Edwin Pozharski wrote:
>>
>> In the absence of such you can resort to carefully bending the loop or bending the pin (Jim Holton made a nifty device for bending the pin) while keeping the xtal bathed in the cold stream.
>>
>>
>> I would also mention these
>>
>> https://hamptonresearch.com/product-Adjustable-Mounted-CryoLoop-385.html
>>
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