Hi, I'm meant to know this but I'm blanking, so I'll crowdsource instead:
Anybody know a (the) reference where it was showed that the best SAD
data is obtained by collecting multiple revolutions at different crystal
offsets (kappa settings)? It's axiomatic now (I hope!), but I remember
seeing someone actually show this. I thought Sheldrick early tweens,
but PubMed is not being useful.
(Oh dear, this will unleash references from the 60s, won't it.)
phx
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