Hello,
I have a SeMet-SAD dataset (at Br edge : 2.7 A) and a 2 wavelength MAD
dataset (inflexion and remote : 3 A). The SAD dataset when searched for
heavy atom sites with a native dataset (SIRAS) gives a figure of merit of
0.26 and Z-score of 28. The MAD dataset by itself gives a low figure of
merit (~0.18).
My question is :
How can I use the good sites from the SAD dataset for their refinement using
SOLVE iwith the MAD dataset? There is a keyword in SOLVE named 'REFINEALL'
but I am not sure if it helping me. If I try to use the keyword, along with
SCALE_MAD and ANALYZE_SOLVE, it reduces the number of sites and gives a low
figure of merit.
Any suggestions on this will be appreciated.
With Regards,
Ankit
|