Dear all,

 

Thanks to Vincent, Eleanor, herman and others! It turns out I’ve managed to sort it out a different way – the initial TFZ of 10 with cutout density and resultant map was a bit underwhelming and indicative of an issue – so I cut my ~140ang long molecule in half and searched with density of those halves...TFZ increases to 19 and I can now see (and place) the first half well, with the remainder flexing. I’ll now use these two placed crystal forms in averaging. A good lesson for me that a tube shaped molecule can bend between forms

 

Thanks again

Andy

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