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Dear Dean,
I appreciate you might not be able to reveal further details but 'disappearing >>during<< data collection' sounds interesting as does 'metals' plural (are they expected to be close together?). 
Best wishes,
John

Prof John R Helliwell DSc
 
 

On 30 Apr 2014, at 11:33, Dean Derbyshire <[log in to unmask]> wrote:

> Hi all,
> Has anyone experienced catalytic metal ions disappearing during data collection ?
> If so, is there a way of preventing it?
> D.
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