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Dear All,


I have a small molecule single crystal. I want to solve its structure by x-ray diffraction.


Could you please teach me how to collect the diffraction data?


I have some experience with protein crystals. But it's the first time for small molecule.
I don't how to set the parameters, like oscillating angle.
And are there any key points I should pay special attention to?


Thanks in advance!
Pengfei