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Hi, > Thanks for your help and for sending the tutorial links. Since yesterday, I've been able to assign at least some of the spin systems beginning in either the tocsy or hsqc experiments. I am still running into occasional difficulty changing a resonance number to its chemical shift-based atom identity (e.g., [161] instead of MetHg) on the tocsy. Under the "edit assignment" pop-up, I click on the "set atom type" but when I click on the correct atom (e.g., 574MetHg) on the "browse atoms" pop-up, this input is not reflected on the assignment in the "edit assignment" pop-up. This has only happened a couple of times and I am not sure why. Usually, I can set the atom type. Something like this can happen when you select one assignment, realize it is wrong, cancel and click on something else instead. After canceling an assignment the popup remains present but no longer seems connected to the edit assignment window. In this case you just have to close it and try again. Patrick