For info. I suspect that this is only an issue if an indirect NOESY type
experiment is made in v2.1 before moving to v2.2 (where we deal with them
properly).
---------- Forwarded message ----------
Date: Thu, 14 Jul 2011 12:55:34 +0100 (BST)
From: Tim Stevens <[log in to unmask]>
Subject: Re: Making distance restraints
> I am able to make distance restraints without trouble for the first
> 2 experiments by clicking the Make assigned restraints button, but
> this does not work for the 15N,13C HSQC-NOESY-HSQC experiment even
> though I have peaks assigned.
Turns out this was fairly easy to solve. In the
Experiments::Experiments:Experiment Types panel set the Full Type column for
the HSQC-NOESY-HSQC experiment to None and then back to
"h[C]_H[N].though-space" again. After doing this distance restrains can be made
in the usual way.
For some reason, perhaps due to the move to v2.2, the indirect 'through-space'
transfer (between 13C and 1H) was missing, as displayed in the Dim-Dim Transfer
table. Hence, the experiment type needed to be reset.
Regards,
Tim
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Dr Tim Stevens Email: [log in to unmask]
Department of Biochemistry [log in to unmask]
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United Kingdom http://www.ccpn.ac.uk
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