Hello,
Tim suggests unsetting the experiment type (i.e. to none) and then
resetting it. If this still doesn't work he'd like to see the project.
(Also, he assumes this experiment has HHC dimensions not HCC.)
Wayne
On Thu, 11 Nov 2010, mas caroline wrote:
> Hi all,
>
> I have a problem with a 13C-13C HMQC-NOESY-HMQC.
> I am not able to convert my Peak-list into distance restraints.
> In Structure: Make Distance Restraints, when I click on "Make Assigned Restraints"
> nothing appends...
>
> In Experiments: Experiments, the category is set as "through-space" and in Type
> Synonym, the experiment type as: 13C,13C HSQC-NOESY-HSQC.
> But I noticed that in the Dim-Dim transfer, there is just the "onebond" type
> between 1H and 13C, and there is no NOESY transfer.
> This might be the reason why it can't make Restraints.
>
> How can the NOESY Dimension Transfer can be added in the Dim-Dim?
>
> Is it possible that the problem is due to the fact that NOEs observed in this
> experiment are between H and C atoms, it would recognize as H-C distance restraints
> and not as the usual distances between two H?
>
> Thanks in advance.
>
> Caroline
>
> --
> Centre for Advanced Imaging
> School of Chemistry and Molecular Biosciences
> The University of Queensland
> St. Lucia, QLD, Australia
> http://www.scmb.uq.edu.au
>
>
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