Hi,
On Thu, May 22, 2008 at 11:22:19AM -0700, Juergen Bosch wrote:
> You can also scratch your head and look at the selfrotation function
> of your dataset.
Some of that scratching can be done using GETAX for you - it's in CCP4
(for years), but hasn't got a CCP4i interface (yet: next release will
have one). If you need help with that, please let me know ...
We used GETAX once in about 1997 with a TaBr-cluster derivative
(single site, phase information to about 7A) SIRAS, having 20
molecules/asu (2.5 D4 octamers) ... You do need to have a Cn/Dn local
NCS though ...
> You might also try out using only the peak dataset (peak & inflection)
> and see if the other wavelength actually harm your electrondensity,
> furthermore you could use Sharp to optimize your phases first.
Yes, you want to start with the best density map possible :-)
Cheers
Clemens
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