On Tue, 18 Sep 2007, Kaare Teilum wrote:
> I have set up the project so that I have one 'Experiment' with all my HSQC
> with the different decoupling powers that I want to calibrate. For each HSQC
> I then have two peak-lists, one for the left and one for the right part of
> each doublet.
At first glance, the way you've set things up is not helping you probably.
The conception behind the Experiment/Spectra distinction (which perhaps
needs to be made clearer to the user) is that one Experiment maps to one
set of data recorded, while the Spectra within it are different instances
of the processing of that data. You almost certainly want your separate
HSQCs in separate Experiments so that you can associate them with
different ShiftLists - this will get around the assignment tolerances that
are preventing your 1H being reassigned to the shifted crosspeaks that lie
outside of the range allowed (or you could change the tolerances for a
quick fix).
--
Dr. Brian O. Smith ---------------------- B Smith at bio gla ac uk
Division of Biochemistry & Molecular Biology,
Institute Biomedical & Life Sciences,
Joseph Black Building, University of Glasgow, Glasgow G12 8QQ, UK.
Tel: 0141 330 5167/6459/3089 Fax: 0141 330 8640
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