Hi Jackie,
It seems that when the crystal structure of L-alanosine was solved, it was done from a solution made by adding conc. HCl (20 ul) to the compound in water (200 ul).
See ref. in Acta Cryst., 1986, C42, 733-738.
I don't know what the starting pH of the compound in water will be, but I think you can try the above ratio or else try to get the pH between 8-9.
Thanks,
Debanu.
________________________________
From: CCP4 bulletin board on behalf of Jacqueline Vitali
Sent: Thu 7/5/2007 6:12 PM
To: [log in to unmask]
Subject: [ccp4bb] L-alanosine
Dear colleagues,
Does anyone know how to dissolve L-alanosine? It is not very soluble in water.
Thanks.
Jackie Vitali
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